3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate

Base Information

• Chemical Name: 3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate
• CAS No.: 1026504-95-9
• Molecular Formula: C₂₂H₂₆N₂O₅S₂
• Molecular Weight: 462.591

Synonyms:3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate

Chemical Property of 3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate

Chemical Property:

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Technology Process of 3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate

There total 2 articles about 3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

p-toluenesulfonyl chloride (98-59-9) + 5-dimethylamino-naphthalene-1-sulfonic acid (3-hydroxy-propyl)-amide (81253-23-8) → 3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate (1026504-95-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 50h;

DOI:10.1039/c8md00562a

Reference yield:

5-(dimethylamino)naphth-1-ylsulfonyl chloride (605-65-2) → 3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate (1026504-95-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 20 °C

2: Et₃N / CH₂Cl₂ / -20 - 0 °C

With triethylamine; In dichloromethane;

DOI:10.1021/jo015658p

Reference yield:

1-(4-fluorobenzyl)-N-(piperidin-4-yl)-1H-benzo[d]imidazol-2-amine hydrobromide + 3-((5-(dimethylamino)naphthalene)-1-sulfonamido)propyl 4-methylbenzenesulfonate (1026504-95-9) → C34H39FN6O2S

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 80 ℃; for 18h;

DOI:10.1039/c8md00562a

upstream raw materials:

p-toluenesulfonyl chloride

5-dimethylamino-naphthalene-1-sulfonic acid (3-hydroxy-propyl)-amide

5-(dimethylamino)naphth-1-ylsulfonyl chloride

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