2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside

Base Information

Chemical Name:2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside
CAS No.:1412408-52-6
Molecular Formula:C₂₉H₄₁F₃O₁₁S
Molecular Weight:654.699
Hs Code.:

Synonyms:2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside

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Chemical Property of 2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside

Chemical Property:

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Technology Process of 2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside

There total 3 articles about 2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1412408-51-5
2',2',2'-Trifluoroethyl 6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 1412408-52-6
2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.carres.2012.08.010 DOI:10.1016/j.carres.2012.08.010

Reference yield:

: 29074-00-8
2,2,2-Trifluoroethyl β-D-glucopyranoside

: 1412408-52-6
2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 72 h / 0 - 20 °C / Inert atmosphere

2: pyridine / 20 °C / Inert atmosphere

With pyridine;
DOI:10.1016/j.carres.2012.08.010 DOI:10.1016/j.carres.2012.08.010

Reference yield:

: 2280-44-6
D-Glucose

: 1412408-52-6
2',2',2'-Trifluoroethyl 2,3,4-tri-O-acetyl-6-O-(2,4,6-trisisopropybenzenesulfonyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride / 0.17 h / 160 °C / Microwave irradiation

2: pyridine / 72 h / 0 - 20 °C / Inert atmosphere

3: pyridine / 20 °C / Inert atmosphere

With pyridine; acetyl chloride;
DOI:10.1016/j.carres.2012.08.010 DOI:10.1016/j.carres.2012.08.010