(1R,4S,5S)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.0^2,7]undeca-2,6-diene

Base Information

• Chemical Name: (1R,4S,5S)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.0^2,7]undeca-2,6-diene
• CAS No.: 287379-86-6
• Molecular Formula: C₂₄H₂₆N₂
• Molecular Weight: 342.484

Synonyms:(1R,4S,5S)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.0^2,7]undeca-2,6-diene

Chemical Property of (1R,4S,5S)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.0^2,7]undeca-2,6-diene

Chemical Property:

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Technology Process of (1R,4S,5S)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.0^2,7]undeca-2,6-diene

There total 1 articles about (1R,4S,5S)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.0^2,7]undeca-2,6-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-camphorquinone (10334-26-6) + rac-1,2-diphenylethylene-1,2-diamine (951-87-1,5700-60-7,16635-95-3,29841-69-8,35132-20-8,107133-00-6) → (1R,4R,5R)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.02,7]undeca-2,6-diene (287379-87-7) + (1R,4S,5S)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.02,7]undeca-2,6-diene (287379-86-6)

Guidance literature:

In benzene; for 17h; Heating;

DOI:10.1016/j.bmc.2007.11.021

Reference yield: 63.0%

(1R,4S,5S)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.02,7]undeca-2,6-diene (287379-86-6) → (1R,2S,4S,5S,7R)-4,5-diphenyl-1,11,11-trimethyl-3,6-diazatricyclo[6.2.1.02,7]undecane

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 4h;

DOI:10.1021/jo0002137

upstream raw materials:

(R)-camphorquinone

rac-1,2-diphenylethylene-1,2-diamine

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