2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol

Base Information

Chemical Name:2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol
CAS No.:1352408-14-0
Molecular Formula:C₅₉H₇₇N₃O₈
Molecular Weight:956.276
Hs Code.:

Synonyms:2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol

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Chemical Property of 2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol

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Technology Process of 2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol

There total 4 articles about 2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 951767-71-8
2-azido-3,4-di-O-benzyl-1-O-(2,3-di-O-benzyloxyl-4,6-O-benzyllidene-α-D-galactopyranosyl)-D-ribooctadecane-1,3,4-triol

: 1352408-14-0
2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol

Guidance literature:: With borane-THF; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1039/c1ob06235b

Reference yield: 70.0%

: C₆₅H₉₁N₃O₈Si

: 1352408-14-0
2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol

: C₅₉H₇₇N₃O₈

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 202812-10-0
(2S,3S,4S)-2-azido-3,4-di-O-benzyl-octadecan-1,3,4-triol

: 1352408-14-0
2-azido-3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)octadecane-1,3,4-triol

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran / 1 h / -20 °C

2: borane-THF; copper(II) bis(trifluoromethanesulfonate) / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With borane-THF; trimethylsilyl trifluoromethanesulfonate; copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1ob06235b