3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

Base Information

Chemical Name:3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol
CAS No.:1352408-20-8
Molecular Formula:C₃₆H₆₃NO₈
Molecular Weight:637.898
Hs Code.:

Synonyms:3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

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Chemical Property of 3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

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Technology Process of 3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

There total 7 articles about 3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1352408-17-3
3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-6-hydroxy-6-iodo-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

: 1352408-20-8
3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

Guidance literature:: With hydrogen; palladium; In methanol; at 20 ℃; under 760.051 Torr;
DOI:10.1039/c1ob06235b

Reference yield:

: 1352408-15-1
3,4-di-O-benzyl-1-O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

: 1352408-20-8
3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / toluene / 0.17 h / Inert atmosphere; Reflux

1.2: 0.33 h / 80 °C / Inert atmosphere; Reflux

2.1: hydrogen; palladium / methanol / 20 °C / 760.05 Torr

With hydrogen; palladium; triphenylphosphine; In methanol; toluene;
DOI:10.1039/c1ob06235b

Reference yield:

: C₅₉H₇₉NO₈

: 1352408-20-8
3,4-dihydroxy-1-O-(3,4,5-trihydroxy-α-D-galactopyranosyl)-2-(6-phenylhexanoyl)aminooctadecane-1,3,4-triol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

2.1: triphenylphosphine / toluene / 0.17 h / Inert atmosphere; Reflux

2.2: 0.33 h / 80 °C / Inert atmosphere; Reflux

3.1: hydrogen; palladium / methanol / 20 °C / 760.05 Torr

With hydrogen; palladium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; In methanol; dichloromethane; toluene;
DOI:10.1039/c1ob06235b