(Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile

Base Information

Chemical Name:(Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile
CAS No.:1027370-83-7
Molecular Formula:C₂₅H₂₄N₂O₃
Molecular Weight:400.477
Hs Code.:

Synonyms:(Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile

Chemical Property:

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Technology Process of (Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile

There total 1 articles about (Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium; 3-formyl-4-methoxy-phenolate

: 1027370-83-7
(Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 1.91 g / dimethylformamide / 20 h / 20 °C

2: NaOMe / dimethylsulfoxide / 0.33 h / 100 °C

3: ethanol / 1 h / Heating

With sodium methylate; In ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm010407u

Reference yield: 61.0%

: 50-01-1
guanidine hydrochloride

: 1027370-83-7
(Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile

: 397245-85-1
2,4-diamino-5-[2-methoxy-5-(4-methoxybenzyloxy)benzyl]pyrimidine

Guidance literature:: guanidine hydrochloride; With sodium ethanolate; In ethanol; for 0.0833333h;

(Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile; In ethanol; for 20h; Further stages.; Heating;
DOI:10.1021/jm010407u

Reference yield:

: 1027370-83-7
(Z)-2-[2-Methoxy-5-(4-methoxy-benzyloxy)-benzyl]-3-phenylamino-acrylonitrile

: 397245-73-7
2,4-diamino-5-(2-methoxy-5-hydroxybenzyl)pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOEt / ethanol / 0.08 h

1.2: 61 percent / ethanol / 20 h / Heating

2.1: 89 percent / TsOH*H₂O / methanol / 48 h / 20 °C

With sodium ethanolate; toluene-4-sulfonic acid; In methanol; ethanol;
DOI:10.1021/jm010407u