4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

Base Information

Chemical Name:4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline
CAS No.:1070910-93-8
Molecular Formula:C₄₆H₇₃NO₂Sn
Molecular Weight:790.801
Hs Code.:

Synonyms:4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

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Chemical Property of 4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

Chemical Property:

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Technology Process of 4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

There total 4 articles about 4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1070910-91-6
N,N-bis(4-octyloxyphenyl)-4-bromophenylamine

: 1461-22-9
tributyltin chloride

: 1070910-93-8
4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

Guidance literature:: N,N-bis(4-octyloxyphenyl)-4-bromophenylamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

tributyltin chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.chempr.2019.07.015

Reference yield:

: 540-38-5
p-Iodophenol

: 1070910-93-8
4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / Inert atmosphere; Reflux

2.1: 1,10-Phenanthroline; copper(l) iodide; potassium hydroxide / toluene / 24 h / Inert atmosphere; Reflux

3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

With copper(l) iodide; n-butyllithium; 1,10-Phenanthroline; potassium carbonate; potassium hydroxide; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.chempr.2019.07.015

Reference yield:

: 96693-06-0
4-(n-octyloxy)-iodobenzene

: 1070910-93-8
4-(octyloxy)-N-(4-(octyloxy)phenyl)-N-(4-(tributylstannyl)phenyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,10-Phenanthroline; copper(l) iodide; potassium hydroxide / toluene / 24 h / Inert atmosphere; Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

With copper(l) iodide; n-butyllithium; 1,10-Phenanthroline; potassium hydroxide; In tetrahydrofuran; hexane; toluene;
DOI:10.1016/j.chempr.2019.07.015