N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide

Base Information

Chemical Name:N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide
CAS No.:1155286-93-3
Molecular Formula:C₂₃H₂₀ClFN₄OS
Molecular Weight:454.955
Hs Code.:

Synonyms:N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide

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Technology Process of N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide

There total 1 articles about N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1118-68-9
dimethylaminoacetic acid

: 1155286-91-1
5-[4-(3-chloro-phenyl)-5-fluoro-benzothiazol-6-ylmethyl]-pyridin-2-ylamine

: 1155286-93-3
N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide

Guidance literature:: dimethylaminoacetic acid; With thionyl chloride; In dichloromethane; for 3h;

5-[4-(3-chloro-phenyl)-5-fluoro-benzothiazol-6-ylmethyl]-pyridin-2-ylamine; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; for 3h;

Reference yield: 98.0%

: 1155286-93-3
N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide

: 1155286-92-2
N-{5-[4-(3-chloro-phenyl)-5-fluoro-benzothiazol-6-ylmethyl]-pyridin-2-yl}-2-dimethylamino-acetamide Hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; for 1h;

Reference yield: 19.0%

: 1155286-93-3
N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide

: 1155287-06-1
N-oxide N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide

Guidance literature:: N-{5-[4-(3-chlorophenyl)-5-fluorobenzothiazol-6-ylmethyl]pyridin-2-yl}-2-dimethylaminoacetamide; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 2h;

With potassium carbonate; In dichloromethane; water;