1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt

Base Information

Chemical Name:1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt
CAS No.:1234307-07-3
Molecular Formula:C₃₀H₃₅O₉S*Na
Molecular Weight:594.658
Hs Code.:

Synonyms:1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt

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Chemical Property of 1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt

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Technology Process of 1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt

There total 17 articles about 1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.7%

: 1105543-59-6
1-O-(2',3',4'-tri-O-benzyl-6'-thioacetyl-α-D-quinovosyl)propane-1,3-diol

: 1234307-07-3
1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt

Guidance literature:: 1-O-(2',3',4'-tri-O-benzyl-6'-thioacetyl-α-D-quinovosyl)propane-1,3-diol; With Oxone; potassium acetate; acetic acid; at 20 ℃; for 48h;

With sodium methylate; In methanol; at 20 ℃; for 3h;

Reference yield: 88.0%

: 1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)-3-O-p-methoxybenzylpropane-1,3-diol sodium salt

: 1234307-07-3
1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1.5h;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 1234307-07-3
1-O-(2,3,4-tri-O-benzyl-6-sulfo-α-D-glucopyranosyl)propane-1,3-diol sodium salt

Guidance literature:: Multi-step reaction with 7 steps

1.1: trifluorormethanesulfonic acid / 48 h / 0 - 80 °C

1.2: 4 h / 40 °C

2.1: sodium hydroxide / N,N-dimethyl-formamide / 24 h / 20 °C

3.1: lithium aluminium tetrahydride; aluminum (III) chloride / dichloromethane; diethyl ether / 4 h / Reflux

4.1: dmap; pyridine / 16 h / 20 °C

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 11 h / 0 - 20 °C / Inert atmosphere

5.2: 13 h / 0 - 20 °C

6.1: N,N-dimethyl-formamide / 3 h / 90 °C

7.1: Oxone; potassium acetate; acetic acid / 48 h / 20 °C

7.2: 3 h / 20 °C

With pyridine; dmap; aluminum (III) chloride; Oxone; lithium aluminium tetrahydride; trifluorormethanesulfonic acid; potassium acetate; acetic acid; 9-bora-bicyclo[3.3.1]nonane; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;