S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide

Base Information

Chemical Name:S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide
CAS No.:156977-61-6
Molecular Formula:C₁₆H₂₅NO₃S₂Si
Molecular Weight:371.597
Hs Code.:

Synonyms:S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide

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Chemical Property of S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide

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Technology Process of S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide

There total 3 articles about S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 108-98-5
thiophenol

: 156977-60-5
<2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>acetic acid 1,1-dioxide

: 156977-61-6
S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; for 1h; Ambient temperature;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 156977-61-6
S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium / 1.) THF, hexane, -78 deg C, 2 min, 2.) THF, hexane, -78 deg C, 15 min

2: 100 percent / H₂ / 10percent Pd/C / ethanol / 0.5 h / Ambient temperature

3: 86 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 1 h / Ambient temperature

With n-butyllithium; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethanol;

Reference yield:

: 156977-59-2
benzyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>acetate 1,1-dioxide

: 156977-61-6
S-phenyl <2-(tert-butyldimethylsilyl)-1,2-thiazetidin-3-yl>thioacetate 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 10percent Pd/C / ethanol / 0.5 h / Ambient temperature

2: 86 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 1 h / Ambient temperature

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethanol;