ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate

Base Information

Chemical Name:ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate
CAS No.:256477-73-3
Molecular Formula:C₁₈H₂₀Cl₂N₂O₄S
Molecular Weight:431.34
Hs Code.:

Synonyms:ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate

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Chemical Property of ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate

Chemical Property:

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Technology Process of ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate

There total 4 articles about ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 223671-80-5
1,4-dichloro-7-isoquinolinesulphonyl chloride

: 1678-68-8
ethyl trans-4-aminocyclohexanecarboxylate

: 256477-73-3
ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 491-30-5
1-isoquinolone

: 256477-73-3
ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide / acetonitrile

2: triethylamine / dichloromethane

With N-chloro-succinimide; triethylamine; In dichloromethane; acetonitrile;

Reference yield:

: 223671-81-6
4-chloro-1-oxo-1,2-dihydro-7-isoquinolinesulfonyl chloride

: 256477-73-3
ethyl trans-4-{[(1,4-dichloro-7-isoquinolinyl)sulphonyl]amino}cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / diethyl ether; acetonitrile

2: triethylamine / dichloromethane

With triethylamine; trichlorophosphate; In diethyl ether; dichloromethane; acetonitrile;