(4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal

Base Information

Chemical Name:(4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal
CAS No.:122213-56-3
Molecular Formula:C₂₆H₂₅NO₄
Molecular Weight:415.489
Hs Code.:

Synonyms:(4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal

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Chemical Property of (4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal

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Technology Process of (4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal

There total 5 articles about (4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122213-51-8
N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide

: 122213-56-3
(4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Et₃N / toluene / 0.25 h / 0 °C

2: 62 percent / LiAlH₄ / tetrahydrofuran / 0.25 h / -78 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1021/jo00277a016

Reference yield:

: 122213-53-0
(4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxylic acid isoxazolidide

: 122213-56-3
(4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / LiAlH₄ / tetrahydrofuran / 0.25 h / -78 °C

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1021/jo00277a016

Reference yield:

: 122213-50-7
N-(9-phenylfluoren-9-yl)-L-serine

: 122213-56-3
(4S)-2-oxo-3-(9-phenylfluoren-9-yl)oxazolidine-4-carboxaldehyde Isopropyl hemiacetal

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / 1.) hydroxybenzotriazide monohydrate, 2.) dicyclohexylcarbodiimide / tetrahydrofuran; dimethylformamide; H₂O / 18 h / 0 °C

2: 99 percent / Et₃N / toluene / 0.25 h / 0 °C

3: 62 percent / LiAlH₄ / tetrahydrofuran / 0.25 h / -78 °C

With lithium aluminium tetrahydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo00277a016