N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide

Base Information

Chemical Name:N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide
CAS No.:122213-51-8
Molecular Formula:C₂₅H₂₄N₂O₃
Molecular Weight:400.477
Hs Code.:

Synonyms:N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide

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Chemical Property of N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide

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Technology Process of N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide

There total 2 articles about N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 504-72-3
isoxazolidine

: 122213-50-7
N-(9-phenylfluoren-9-yl)-L-serine

: 122213-51-8
N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 0 ℃; for 18h;
DOI:10.1021/jo00277a016

Reference yield:

: C₂₈H₃₅NO₃Si₂

: 122213-51-8
N-(9-phenylfluoren-9-yl)-L-serine isoxazolidide

Guidance literature:: Multi-step reaction with 2 steps

1: 5percent citric acid/H₂O / tetrahydrofuran / 0.08 h

2: 80 percent / 1.) hydroxybenzotriazide monohydrate, 2.) dicyclohexylcarbodiimide / tetrahydrofuran; dimethylformamide; H₂O / 18 h / 0 °C

With water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; citric acid; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00277a016