3-Chloro-2,2,3,3-tetrafluoropropanoyl chloride

Base Information

• Chemical Name: 3-Chloro-2,2,3,3-tetrafluoropropanoyl chloride
• CAS No.: 24503-62-6
• Molecular Formula: C₃Cl₂F₄O
• Molecular Weight: 198.932
• Hs Code.: 2915900090
• European Community (EC) Number: 833-372-5
• DSSTox Substance ID: DTXSID20382118
• Nikkaji Number: J60.929C
• Wikidata: Q82173428
• Mol file: 24503-62-6.mol

Synonyms:24503-62-6;3-chloro-2,2,3,3-tetrafluoropropanoyl chloride;3-Chlorotetrafluoropropionyl chloride;MFCD00153100;3-CHLOROTETRAFLUOROPROPIONYLCHLORIDE;Propanoyl chloride, 3-chloro-2,2,3,3-tetrafluoro-;3-Chlorotetrafluoropropanoyl chloride;AMINOETHYLPHOSPHINICACID;Propanoyl chloride,3-chloro-2,2,3,3-tetrafluoro-;SCHEMBL3282267;DTXSID20382118;3-Chlorotetrafluoropropanyl chloride;AKOS005258176;AT22448;FT-0676252;3-Chloro-2,2,3,3-tetrafluoropropionyl chloride;A817339;3-chloranyl-2,2,3,3-tetrakis(fluoranyl)propanoyl chloride

Chemical Property of 3-Chloro-2,2,3,3-tetrafluoropropanoyl chloride

Chemical Property:

• Vapor Pressure: 166mmHg at 25°C
• Refractive Index: 1.3380 (589.3 nm 26℃)
• Boiling Point: 64.2°Cat760mmHg
• Flash Point: °C
• PSA: 17.07000
• Density: 1.66g/cm³
• LogP: 2.21870
• Sensitive.: Moisture Sensitive
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 197.9262327
• Heavy Atom Count: 10
• Complexity: 157

Purity/Quality:

99%, ^*data from raw suppliers

3-ChlorotetrafluoropropanoylChloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 34
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(=O)(C(C(F)(F)Cl)(F)F)Cl

Technology Process of 3-Chloro-2,2,3,3-tetrafluoropropanoyl chloride

There total 3 articles about 3-Chloro-2,2,3,3-tetrafluoropropanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

freon-214 (2268-46-4) → 2,2,3,3-tetrafluoro-3-chloropropionyl chloride (24503-62-6) + 2-chlorotetrafluoropropionyl chloride (6066-46-2)

Guidance literature:

With sulfuric acid; sulfur trioxide; silver nitrate; mercury(II) oxide; for 8h; Title compound not separated from byproducts; Heating;

DOI:10.1016/S0022-1139(00)82397-0

Reference yield:

tri(2,2,3,3-tetrafluoro-1,1,3-trichloropropyl) phosphate (24503-61-5) → 2,2,3,3-tetrafluoro-3-chloropropionyl chloride (24503-62-6)

Guidance literature:

Multistep reaction; (i) KF, (ii) AlCl₃;

Reference yield:

2,2,3,3-tetrafluoro-1,1,3-trichloropropyl 2,2,3,3-tetrafluoro-3-chloropropionate (168554-73-2) → 2,2,3,3-tetrafluoro-3-chloropropionyl chloride (24503-62-6)

Guidance literature:

at 180 ℃;

upstream raw materials:

tri(2,2,3,3-tetrafluoro-1,1,3-trichloropropyl) phosphate

freon-214

2,2,3,3-tetrafluoro-1,1,3-trichloropropyl 2,2,3,3-tetrafluoro-3-chloropropionate

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