(R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane

Base Information

Chemical Name:(R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane
CAS No.:613668-24-9
Molecular Formula:C₃₁H₃₉N₃O₆S₃
Molecular Weight:645.865
Hs Code.:

(R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0<sup>1,9</sup>>tridecane

Synonyms:(R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane

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Chemical Property of (R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane

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Technology Process of (R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane

There total 3 articles about (R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 16695-22-0
N,N-bis(tosyloxyethyl)-p-toluenesulfonamide

: 143585-47-1
(R,R)-1,2-bis(tosylamino)cyclohexane

: 613668-24-9
(R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane

Guidance literature:: (R,R)-1,2-bis(tosylamino)cyclohexane; With lithium hydride; In N,N-dimethyl-formamide; at 70 ℃;

N,N-bis(tosyloxyethyl)-p-toluenesulfonamide; In N,N-dimethyl-formamide; at 50 ℃; Further stages.;
DOI:10.1039/b716938h

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 613668-24-9
(R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / pyridine / 2 h / 0 °C

2: 28 percent / K₂CO₃ / dimethylformamide / 168 h / 50 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/a809125k

Reference yield:

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 613668-24-9
(R,R)-2,5,8-tris(p-tolylsulfonyl)-2,5,8-triazabicyclo<7.4.0^1,9>tridecane

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / NaOH / H₂O; diethyl ether / 4.75 h

2: 28 percent / K₂CO₃ / dimethylformamide / 168 h / 50 °C

With sodium hydroxide; potassium carbonate; In diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1039/a809125k