3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione
CAS No.:905854-85-5
Molecular Formula:C₂₃H₂₀N₂O₃S₆
Molecular Weight:564.819
Hs Code.:

3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-<i>b</i>][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1<i>H</i>-pyrimidine-2,4-dione

Synonyms:3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione

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Chemical Property of 3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione

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Technology Process of 3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione

There total 3 articles about 3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 905854-83-3
N³-benzoyl-N¹-n-butyl-5-iodouracil

: 97307-49-8
ethylenedithiotetrathiafulvalene

: 905854-85-5
3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione

Guidance literature:: ethylenedithiotetrathiafulvalene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

With tributyltin chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;

N³-benzoyl-N¹-n-butyl-5-iodouracil; With copper(l) iodide; tris-(o-tolyl)phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 27h;
DOI:10.1021/jo060748l

Reference yield:

: 705-06-6
1-n-butyluracil

: 905854-85-5
3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: ICl

2.1: 96 percent / pyridine / acetonitrile / 24 h / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

3.2: Bu₃SnCl / tetrahydrofuran; hexane / -78 - 20 °C

3.3: CuI; (o-Tol)3P / Pd(PPh₃)4 / tetrahydrofuran / 27 h / 20 °C

With pyridine; n-butyllithium; Iodine monochloride; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1021/jo060748l

Reference yield:

: 444990-52-7
1-(1-butyl)-5-iodopyrimidine-2,4(1H,3H)-dione

: 905854-85-5
3-benzoyl-1-butyl-5-[2-(5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiin-2-ylidene)-[1,3]dithiol-4-yl]-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / pyridine / acetonitrile / 24 h / 20 °C

2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: Bu₃SnCl / tetrahydrofuran; hexane / -78 - 20 °C

2.3: CuI; (o-Tol)3P / Pd(PPh₃)4 / tetrahydrofuran / 27 h / 20 °C

With pyridine; n-butyllithium; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1021/jo060748l