1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione)

Base Information

Chemical Name:1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione)
CAS No.:947395-33-7
Molecular Formula:C₃₀H₂₂N₄O₆
Molecular Weight:534.528
Hs Code.:

Synonyms:1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione)

Chemical Property:

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Technology Process of 1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione)

There total 3 articles about 1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917081-96-0
3-benzoyl-1-(4-iodophenyl)-5-methylpyrimidine-2,4(1H,3H)-dione

: 947395-33-7
1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione)

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / KOAc / Pd(OAc)2 / dimethylformamide / 3 h / 60 °C

2: polymer-supported benzeneboronic acid; aq. HCl / acetonitrile / 18 h / 20 °C

3: 157 mg / Cu(OAc)2; pyridine; air / CH₂Cl₂ / 48 h / 20 °C

With pyridine; hydrogenchloride; copper diacetate; air; potassium acetate; palladium diacetate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; 3: Chan-Lam-Evans reaction;
DOI:10.1021/ol071006x

Reference yield:

: C₁₈H₁₅BN₂O₅

: 4330-20-5
N-3-benzoylthymine

: 947395-33-7
1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione)

Guidance literature:: With pyridine; copper diacetate; air; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/ol071006x

Reference yield:

: 947395-32-6
3-benzoyl-5-methyl-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)pyrimidine-2,4(1H,3H)-dione

: 947395-33-7
1,1'-(1,4-diphenylene)bis(3-benzoyl-5-methylpyrimidine-2,4(1H,3H)-dione)

Guidance literature:: Multi-step reaction with 2 steps

1: polymer-supported benzeneboronic acid; aq. HCl / acetonitrile / 18 h / 20 °C

2: 157 mg / Cu(OAc)2; pyridine; air / CH₂Cl₂ / 48 h / 20 °C

With pyridine; hydrogenchloride; copper diacetate; air; In dichloromethane; acetonitrile; 2: Chan-Lam-Evans reaction;
DOI:10.1021/ol071006x