6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol

Base Information

Chemical Name:6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol
CAS No.:109229-03-0
Molecular Formula:C₂₉H₂₇F₂N₃O
Molecular Weight:471.55
Hs Code.:

Synonyms:6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol

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Chemical Property of 6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol

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Technology Process of 6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol

There total 5 articles about 6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 109229-11-0
2-Phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol; hydrochloride

: 3312-04-7
4-chloro-1,1-bis(4-fluorophenyl)butane

: 109229-03-0
6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol

Guidance literature:: With sodium carbonate; potassium iodide; In butanone; for 100h; Heating;

Reference yield:

: 41276-30-6
C₉H₁₄O₃NC₆H₅

: 109229-03-0
6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / K₂CO₃ / H₂O / 40 °C

2: 45 percent / toluene / 5 h / Heating

3: 90 percent / HCl(conc.) / H₂O / 8 h / Heating

4: 50 percent / Na₂CO₃, KI / butan-2-one / 100 h / Heating

With hydrogenchloride; sodium carbonate; potassium carbonate; potassium iodide; In water; toluene; butanone;

Reference yield:

: 1670-14-0
benzamidine monohydrochloride

: 109229-03-0
6-[4,4-Bis-(4-fluoro-phenyl)-butyl]-2-phenyl-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / K₂CO₃ / H₂O / 40 °C

2: 45 percent / toluene / 5 h / Heating

3: 90 percent / HCl(conc.) / H₂O / 8 h / Heating

4: 50 percent / Na₂CO₃, KI / butan-2-one / 100 h / Heating

With hydrogenchloride; sodium carbonate; potassium carbonate; potassium iodide; In water; toluene; butanone;