N₄,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt

Base Information

• Chemical Name: N₄,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt
• CAS No.: 1193091-02-9
• Molecular Formula: C₆H₁₅N*C₂₃H₂₂N₃O₈P
• Molecular Weight: 600.609

Synonyms:N₄,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt

Chemical Property of N₄,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt

Chemical Property:

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Technology Process of N₄,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt

There total 1 articles about N₄,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

diphenyl hydrogen phosphite (4712-55-4) + N-benzoyl-2'-deoxycytidine 3'-benzoate (51549-49-6) + triethylamine (121-44-8) → N4,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt (1193091-02-9)

Guidance literature:

diphenyl hydrogen phosphite; N-benzoyl-2'-deoxycytidine 3'-benzoate; With pyridine; at 20 ℃; for 1h; Inert atmosphere;

triethylamine; In water;

DOI:10.1016/j.bmc.2009.08.001

Reference yield:

2-[3-(tert-butoxycarbonylamino)propyl]diethyl malonate trifluoroacetic acid salt (1193091-08-5) + N4,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt (1193091-02-9) → C33H39N4O12P

Guidance literature:

N₄,3'-O-dibenzoyl-2'-deoxycytidin-5'-yl hydrogenophosphonate triethylammonium salt; With pyridine; N,O-bis-(trimethylsilyl)-acetamide; at 20 ℃; for 0.5h; Inert atmosphere;

2-[3-(tert-butoxycarbonylamino)propyl]diethyl malonate trifluoroacetic acid salt; With pyridine; triethylamine; In tetrachloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.bmc.2009.08.001

upstream raw materials:

diphenyl hydrogen phosphite

N-benzoyl-2'-deoxycytidine 3'-benzoate

triethylamine

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