(E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester

Base Information

Chemical Name:(E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester
CAS No.:103215-62-9
Molecular Formula:C₄₅H₄₈O₁₆
Molecular Weight:844.867
Hs Code.:

(E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester

Synonyms:(E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester

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Chemical Property of (E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester

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Technology Process of (E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester

There total 1 articles about (E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103215-60-7
(+)-catechin 5-O-β-D-(2''-O-feruloyl-6''-O-p-coumaroyl)-glucopyranoside

: 77-78-1
dimethyl sulfate

: 103215-62-9
(E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester

Guidance literature:: With potassium carbonate; In acetone; for 3h; Yield given; Heating;
DOI:10.1248/cpb.34.643

Reference yield:

: 124-41-4
sodium methylate

: 103215-62-9
(E)-3-(3,4-Dimethoxy-phenyl)-acrylic acid (2S,3R,4S,5S,6R)-2-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-4,5-dihydroxy-6-[(E)-3-(4-methoxy-phenyl)-acryloyloxymethyl]-tetrahydro-pyran-3-yl ester

: 3901-07-3
3-(4-methoxy-phenyl)acrylic acid methyl ester

: 5396-64-5
methyl (E)-3-(3,4-dimethoxyphenyl)acrylate

: 88126-54-9
7,3',4'-tri-O-methyl-(+)-catechin 5-C-β-D-glucopyeanoside

: 103215-63-0
(E)-3-(4-Methoxy-phenyl)-acrylic acid (2R,3S,4S,5R,6S)-6-[(2R,3S)-2-(3,4-dimethoxy-phenyl)-3-hydroxy-7-methoxy-chroman-5-yloxy]-3,4,5-trihydroxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: In methanol; for 0.166667h; Product distribution; Heating; other reaction time and reaction temperature, other amounts of sodium methoxide;
DOI:10.1248/cpb.34.643