(3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate

Base Information

• Chemical Name: (3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate
• CAS No.: 1197988-95-6
• Molecular Formula: C₂₆H₃₉NO₇S
• Molecular Weight: 509.664

Synonyms:(3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate

Chemical Property of (3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate

Chemical Property:

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Technology Process of (3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate

There total 1 articles about (3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(3R,4R)-4-tert-butyl-1-ethyl-5-nitro-3-(pentan-3-yloxy)cyclohex-1-ene-1,4-dicarboxylate + para-thiocresol (106-45-6) → (1S,2R,3S,4R,5S)-4-tert-butyl-1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate (1141364-91-1) + (3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate (1197988-95-6)

Guidance literature:

With triethylamine; In ethanol; at 23 ℃; for 12h;

DOI:10.1002/chem.201001108

Reference yield:

(3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate (1197988-95-6) → (3R,4R,5R)-4-tert-butyl-1-ethyl-5-nitro-3-(pentan-3-yloxy)cyclohex-1-ene-1,4-dicarboxylate + (3R,4R,5S)-4-tert-butyl-1-ethyl-5-nitro-3-(pentan-3-yloxy)cyclohex-1-ene-1,4-dicarboxylate

Guidance literature:

(3S,4R)-4-tert-butyl 1-ethyl-5-nitro-3-(pentan-3-yloxy)-2-(p-tolylthio)cyclohexane-1,4-dicarboxylate; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 23 ℃; for 0.166667h; Inert atmosphere;

With caesium carbonate; In ethanol; at 23 ℃; for 0.333333h; Inert atmosphere;

upstream raw materials:

para-thiocresol

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