(R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide

Base Information

Chemical Name:(R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide
CAS No.:96854-28-3
Molecular Formula:C₃₀H₂₉NO₄P*I
Molecular Weight:625.443
Hs Code.:

Synonyms:(R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide

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Chemical Property of (R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide

Chemical Property:

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Technology Process of (R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide

There total 4 articles about (R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 99259-18-4
(R)-3-Iodo-2-<(methoxycarbonyl)amino>propanoic Acid Benzyl Ester

: 603-35-0
triphenylphosphine

: 96854-28-3
(R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide

Guidance literature:: In toluene; at 50 ℃; for 120h;
DOI:10.1248/cpb.39.1407

Reference yield:

: 1738-80-3
L-serine benzyl ester p-toluenesulfonate hydrochoride

: 96854-28-3
(R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / NaHCO₃ / H₂O / 1.5 h / Ambient temperature

2: 65 percent / pyridine / 3 h / -10 °C

3: 100 percent / NaI / acetone / 72 h / Ambient temperature

4: 97 percent / toluene / 120 h / 50 °C

With pyridine; sodium hydrogencarbonate; sodium iodide; In water; acetone; toluene;
DOI:10.1248/cpb.39.1407

Reference yield:

: 99259-17-3
(S)-N-(Methoxycarbonyl)serine Benzyl Ester

: 96854-28-3
(R)-<2-(Benzyloxycarbonyl)-2-<(methoxycarbonyl)amino>ethyl>triphenylphosphonium Iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / pyridine / 3 h / -10 °C

2: 100 percent / NaI / acetone / 72 h / Ambient temperature

3: 97 percent / toluene / 120 h / 50 °C

With pyridine; sodium iodide; In acetone; toluene;
DOI:10.1248/cpb.39.1407