Technology Process of C31H32N8O
There total 6 articles about C31H32N8O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chloro[2-(dicyclohexylphosphino)-3 ,6-dimethoxy-2’,4’, 6’-triisopropyl- 1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II); 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium t-butanolate;
In
1,4-dioxane; water; tert-butyl alcohol;
at 150 ℃;
under 12929 Torr;
Flow reactor;
DOI:10.1039/c2ob27002a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine; silica gel / dichloromethane / 20 °C / 5171.62 Torr / Flow reactor
1.2: Inert atmosphere; Flow reactor
2.1: sodium t-butanolate; 1,8-diazabicyclo[5.4.0]undec-7-ene; chloro[2-(dicyclohexylphosphino)-3 ,6-dimethoxy-2’,4’, 6’-triisopropyl- 1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II) / water; 1,4-dioxane; tert-butyl alcohol / 150 °C / 12929 Torr / Flow reactor
With
chloro[2-(dicyclohexylphosphino)-3 ,6-dimethoxy-2’,4’, 6’-triisopropyl- 1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II); silica gel; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; sodium t-butanolate;
In
1,4-dioxane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c2ob27002a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine; silica gel / dichloromethane / 20 °C / 5171.62 Torr / Flow reactor
1.2: Inert atmosphere; Flow reactor
2.1: sodium t-butanolate; 1,8-diazabicyclo[5.4.0]undec-7-ene; chloro[2-(dicyclohexylphosphino)-3 ,6-dimethoxy-2’,4’, 6’-triisopropyl- 1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II) / water; 1,4-dioxane; tert-butyl alcohol / 150 °C / 12929 Torr / Flow reactor
With
chloro[2-(dicyclohexylphosphino)-3 ,6-dimethoxy-2’,4’, 6’-triisopropyl- 1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II); silica gel; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; sodium t-butanolate;
In
1,4-dioxane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c2ob27002a