N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide

Base Information

Chemical Name:N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide
CAS No.:1026893-14-0
Molecular Formula:C₁₈H₁₉N₅O
Molecular Weight:321.382
Hs Code.:

Synonyms:N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide

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Technology Process of N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide

There total 5 articles about N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156601-85-3
N-[5-Methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-2-nitro-phenyl]-acetamide

: 1026893-14-0
N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 4h; under 760 Torr; Ambient temperature;
DOI:10.1248/cpb.42.560

Reference yield:

: 65882-96-4
1-hydroxyimino-1-(3-pyridyl)-2-propanone

: 1026893-14-0
N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate / acetic acid / 0.25 h / 100 °C

2: 52.6 percent / P(OEt)3 / dimethylformamide / 80 °C

3: H₂ / 10percent Pd/C / methanol; tetrahydrofuran / 4 h / 760 Torr / Ambient temperature

With ammonium acetate; hydrogen; triethyl phosphite; palladium on activated charcoal; In tetrahydrofuran; methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.42.560

Reference yield:

: 84257-50-1
4-acetamido-2-methyl benzaldehyde

: 1026893-14-0
N-[2-Amino-5-methyl-4-(5-methyl-4-pyridin-3-yl-1H-imidazol-2-yl)-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / HNO₃ fuming / 0.67 h / -40 - -20 °C

2: ammonium acetate / acetic acid / 0.25 h / 100 °C

3: 52.6 percent / P(OEt)3 / dimethylformamide / 80 °C

4: H₂ / 10percent Pd/C / methanol; tetrahydrofuran / 4 h / 760 Torr / Ambient temperature

With ammonium acetate; hydrogen; nitric acid; triethyl phosphite; palladium on activated charcoal; In tetrahydrofuran; methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.42.560