N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate

Base Information

Chemical Name:N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate
CAS No.:82444-64-2
Molecular Formula:C₁₅H₂₈NOSi*ClO₄
Molecular Weight:365.93
Hs Code.:

Synonyms:N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate

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Chemical Property of N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate

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Technology Process of N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate

There total 4 articles about N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 87883-67-8
3--2-propenyl>-amino>cyclohex-2-enone

: 74-88-4
methyl iodide

: 82444-64-2
N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate

Guidance literature:: With silver perchlorate; In acetonitrile; at 0 - 25 ℃; for 24h;
DOI:10.1021/jo00176a002

Reference yield:

: 55998-74-8
3-(methylamino)-2-cyclohexen-1-one

: 82444-64-2
N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaH / tetrahydrofuran / 1h, reflux -> 25 deg C, 24h

2: 93 percent / AgClO₄ / acetonitrile / 24 h / 0 - 25 °C

With silver perchlorate; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00176a002

Reference yield:

: 74532-54-0
3-trimethylsilyl-2-(methylsulphonyloxymethyl)prop-1-ene

: 82444-64-2
N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaH / tetrahydrofuran / 1h, reflux -> 25 deg C, 24h

2: 93 percent / AgClO₄ / acetonitrile / 24 h / 0 - 25 °C

With silver perchlorate; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00176a002