N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Base Information

Chemical Name:N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide
CAS No.:244091-53-0
Molecular Formula:C₁₇H₂₁Cl₃N₂O₅
Molecular Weight:439.723
Hs Code.:

Synonyms:N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide

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Chemical Property of N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide

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Technology Process of N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide

There total 3 articles about N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: C₂₁H₂₄Cl₃N₃O₈

: 244091-53-0
N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Guidance literature:: With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1021/ol990113r

Reference yield:

: 244091-24-5
N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide

: 244091-53-0
N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / DMAP / tetrahydrofuran / 3 h

2: 91 percent / LiOH; aq. H₂O₂ / tetrahydrofuran / 0.5 h / 0 °C

With dmap; lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran;
DOI:10.1021/ol990113r

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 244091-53-0
N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / DMAP / tetrahydrofuran / 3 h

2: 91 percent / LiOH; aq. H₂O₂ / tetrahydrofuran / 0.5 h / 0 °C

With dmap; lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran;
DOI:10.1021/ol990113r