N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Base Information

• Chemical Name: N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide
• CAS No.: 244091-24-5
• Molecular Formula: C₁₆H₁₆Cl₃N₃O₆
• Molecular Weight: 452.679

Synonyms:N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Chemical Property of N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Chemical Property:

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Technology Process of N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide

There total 1 articles about N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,2-trichloroethyl-{[(2-oxo-1,3-oxazolidin-3-yl)carbonyl]diazenyl} formate (244091-10-9) + trimethyl[(Z)-(1-phenyl-1-propenyl)oxy]silane (66323-99-7) → N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide (244091-24-5) + N-((1S)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Guidance literature:

With [Cu(S,S)-t-Bu-box](OTf)2; In tetrahydrofuran; at -78 ℃; for 24h; Further Variations:; Reagents; Temperatures; time; Product distribution;

DOI:10.1021/ol990113r

Reference yield: 95.0%

N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide (244091-24-5) → N-((1R,2S)-2-hydroxy-1-methyl-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide

Guidance literature:

With triethylsilane; In trifluoroacetic acid; at 0 ℃; for 2h;

DOI:10.1021/ol990113r

Reference yield: 92.0%

N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(2-oxo-1,3-oxazolidin-3-yl)carbonylamino](2,2,2-trichloroethoxy)carboxamide (244091-24-5) → N-((4R,5R)-4-methyl-2-oxo-5-phenyl-(1,3-oxazolidin-3-yl))(2-oxo-1,3-oxazolidin-3-yl)carboxamide

Guidance literature:

With L-Selectride; In tetrahydrofuran; at -78 - 20 ℃; for 2h;

DOI:10.1021/ol990113r

upstream raw materials:

2,2,2-trichloroethyl-{[(2-oxo-1,3-oxazolidin-3-yl)carbonyl]diazenyl} formate

trimethyl[(Z)-(1-phenyl-1-propenyl)oxy]silane

Downstream raw materials:

N-((1R)-1-methyl-2-oxo-2-phenylethyl)-N-[(tert-butoxy)carbonylamino](2,2,2-trichloroethoxy)carboxamide

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