(2-(Diethylcarbamoyl)phenyl)boronic acid

Base Information

Chemical Name:(2-(Diethylcarbamoyl)phenyl)boronic acid
CAS No.:129112-21-6
Molecular Formula:C11H16BNO3
Molecular Weight:221.064
Hs Code.:2931900090
DSSTox Substance ID:DTXSID40400580
Nikkaji Number:J1.347.016B
Wikidata:Q82203590
Mol file:129112-21-6.mol

Synonyms:129112-21-6;(2-(Diethylcarbamoyl)phenyl)boronic acid;2-(N,N-Diethylaminocarbonyl)phenylboronic acid;[2-(diethylcarbamoyl)phenyl]boronic Acid;2-(diethylcarbamoyl)phenylboronic acid;2-(Diethylcarbamoyl)benzeneboronic acid;Boronic acid, [2-[(diethylamino)carbonyl]phenyl]-;2-(DIETHYLAMINO)CARBONYLBENZENEBORONIC ACID;SCHEMBL521053;DTXSID40400580;TULUDWZVHWOWHZ-UHFFFAOYSA-N;MFCD01318988;AKOS015838653;AB08799;(2-(Diethylcarbamoyl)phenyl)boronicacid;BS-20632;CS-0176000;F75048;A888908;Boronicacid,b-[2-[(diethylamino)carbonyl]phenyl]-

Suppliers and Price of (2-(Diethylcarbamoyl)phenyl)boronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(2-(diethylcarbamoyl)phenyl)boronicacid
500mg
$ 310.00

SynQuest Laboratories
2-(Diethylcarbamoyl)benzeneboronic acid 95%
1 g
$ 380.00

Crysdot
(2-(Diethylcarbamoyl)phenyl)boronicacid 95+%
1g
$ 164.00

Crysdot
(2-(Diethylcarbamoyl)phenyl)boronicacid 95+%
5g
$ 635.00

American Custom Chemicals Corporation
2-(N,N-DIETHYLAMINOCARBONYL)PHENYLBORONIC ACID 95.00%
1G
$ 319.20

Alichem
(2-(Diethylcarbamoyl)phenyl)boronicacid
5g
$ 522.24

AK Scientific
2-(N,N-Diethylaminocarbonyl)phenylboronicacid
5g
$ 1087.00

AK Scientific
2-(N,N-Diethylaminocarbonyl)phenylboronicacid
1g
$ 281.00

Total 29 raw suppliers

Chemical Property of (2-(Diethylcarbamoyl)phenyl)boronic acid

Chemical Property:

Vapor Pressure:3.13E-08mmHg at 25°C
Melting Point:64-70°C
Refractive Index:1.54
Boiling Point:432 °C at 760 mmHg
Flash Point:215.1 °C
PSA：60.77000
Density:1.14g/cm³
LogP:-0.15160
Storage Temp.:Keep Cold
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:221.1223235
Heavy Atom Count:16
Complexity:231

Purity/Quality:

97% ^*data from raw suppliers

(2-(diethylcarbamoyl)phenyl)boronicacid ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B(C1=CC=CC=C1C(=O)N(CC)CC)(O)O

Technology Process of (2-(Diethylcarbamoyl)phenyl)boronic acid

There total 3 articles about (2-(Diethylcarbamoyl)phenyl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 1696-17-9
N,N-diethylbenzamide

: 129112-21-6
2-(N,N-diethylaminocarbonyl)phenylboronic acid

Guidance literature:: N,N-diethylbenzamide; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 1h;

Trimethyl borate; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃;

With hydrogenchloride; ammonium chloride; In tetrahydrofuran; cyclohexane; pH=5 - 6;
DOI:10.1139/v00-055

Reference yield: 92.0%

: 1696-17-9
N,N-diethylbenzamide

: 129112-21-6
2-(N,N-diethylaminocarbonyl)phenylboronic acid

Guidance literature:: N,N-diethylbenzamide; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;

With Trimethyl borate; In tetrahydrofuran; at 20 ℃;
DOI:10.1139/v03-179

Reference yield:

: 5419-55-6
Triisopropyl borate

: 1696-17-9
N,N-diethylbenzamide

: 129112-21-6
2-(N,N-diethylaminocarbonyl)phenylboronic acid

Guidance literature:: N,N-diethylbenzamide; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 1h; Inert atmosphere;

Triisopropyl borate; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃; for 19.5h; Inert atmosphere;
DOI:10.1021/acs.joc.7b00890