benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside
CAS No.:75869-85-1
Molecular Formula:C₃₅H₄₃NO₁₁
Molecular Weight:653.727
Hs Code.:

Synonyms:benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside

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Chemical Property of benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside

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Technology Process of benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside

There total 6 articles about benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 75869-84-0
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranoside

: 75869-85-1
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside

Guidance literature:: With sodium methylate; In methanol; Ambient temperature;
DOI:10.1016/S0008-6215(00)85566-4

Reference yield:

: 100-39-0
benzyl bromide

: 75869-85-1
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 73.1 percent / 5percent sodium hydroxide / tetrabutylammonium hydrogensulfate / CH₂Cl₂; H₂O / 72 h / Heating

2: tetra-N-methylurea, silver triflate / CH₂Cl₂ / 72 h / Ambient temperature

3: 70 percent / sodium methoxide / methanol / Ambient temperature

With sodium hydroxide; sodium methylate; silver trifluoromethanesulfonate; tetramethylurea; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane; water;
DOI:10.1016/S0008-6215(00)85566-4

Reference yield:

: 75869-82-8
benzyl 2-acetamido-3-O-benzyl-2-deoxy-α-D-galactopyranoside

: 75869-85-1
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-β-D-galactopyranosyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 73.1 percent / 5percent sodium hydroxide / tetrabutylammonium hydrogensulfate / CH₂Cl₂; H₂O / 72 h / Heating

2: tetra-N-methylurea, silver triflate / CH₂Cl₂ / 72 h / Ambient temperature

3: 70 percent / sodium methoxide / methanol / Ambient temperature

With sodium hydroxide; sodium methylate; silver trifluoromethanesulfonate; tetramethylurea; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane; water;
DOI:10.1016/S0008-6215(00)85566-4