(E)-2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)-3-p-tolylacrylonitrile

Base Information

Chemical Name:(E)-2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)-3-p-tolylacrylonitrile
CAS No.:1335203-59-2
Molecular Formula:C₁₆H₁₀Cl₂N₄
Molecular Weight:329.188
Hs Code.:

Synonyms:(E)-2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)-3-p-tolylacrylonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)-3-p-tolylacrylonitrile

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Technology Process of (E)-2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)-3-p-tolylacrylonitrile

There total 2 articles about (E)-2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)-3-p-tolylacrylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1267294-31-4
2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)acetonitrile

: 104-87-0
4-methyl-benzaldehyde

: 1335203-59-2
(E)-2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)-3-p-tolylacrylonitrile

Guidance literature:: With triethylamine; In toluene; for 24h; Reflux;
DOI:10.1016/j.ejmech.2011.06.018

Reference yield:

: 34374-67-9
5,6-dichloro-1H-benzo[d][1,2,3]triazole

: 1335203-59-2
(E)-2-(5,6-dichloro-1H-benzo[d][1,2,3]triazol-1-yl)-3-p-tolylacrylonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / N,N-dimethyl-formamide / 12 h / Reflux

2: triethylamine / toluene / 24 h / Reflux

With triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2011.06.018