[Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine

Base Information

Chemical Name:[Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine
CAS No.:77604-34-3
Molecular Formula:C₂₄H₂₃NO₂
Molecular Weight:357.452
Hs Code.:

Synonyms:[Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine

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Chemical Property of [Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine

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Technology Process of [Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine

There total 4 articles about [Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 14371-10-9
(E)-3-phenylpropenal

: 19293-62-0
p,p'-dimethoxybenzhydrylamine

: 77604-34-3
[Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine

Guidance literature:: With magnesium sulfate; In dichloromethane; at -20 ℃; for 2h;
DOI:10.1139/v87-014

Reference yield:

: 728-87-0
4,4'-Dimethoxybenzhydrol

: 77604-34-3
[Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CH₂Cl₂ / 0.5 h / -50 - -20 °C

2: NH₃ / tetrahydrofuran; CH₂Cl₂ / -50 °C

3: 78 percent / magnesium sulfate / CH₂Cl₂ / 2 h / -20 °C

With ammonia; magnesium sulfate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1139/v87-014

Reference yield:

: 7525-23-7
4,4'-dimethoxydiphenylmethyl chloride

: 77604-34-3
[Bis-(4-methoxy-phenyl)-methyl]-[(E)-3-phenyl-prop-2-en-(E)-ylidene]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: liq. NH₃ / 6 h

2: 4 Angstroem molecular sieves / CH₂Cl₂ / 1.5 h

With 4 A molecular sieve; ammonia; In dichloromethane;
DOI:10.1021/jo00188a026