C₅₀H₅₃N₆O₉PS

Base Information

Chemical Name:C₅₀H₅₃N₆O₉PS
CAS No.:1314716-30-7
Molecular Formula:C₅₀H₅₃N₆O₉PS
Molecular Weight:945.045
Hs Code.:

C<sub>50</sub>H<sub>53</sub>N<sub>6</sub>O<sub>9</sub>PS

Synonyms:C₅₀H₅₃N₆O₉PS

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Chemical Property of C₅₀H₅₃N₆O₉PS

Chemical Property:

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Technology Process of C₅₀H₅₃N₆O₉PS

There total 19 articles about C₅₀H₅₃N₆O₉PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.8%

: 1314716-29-4
C₄₁H₃₆N₄O₈S

: 102691-36-1
N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

: 1314716-30-7
C₅₀H₅₃N₆O₉PS

Guidance literature:: C₄₁H₃₆N₄O₈S; N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite; With 1-methyl-1H-imidazole; 1H-tetrazole; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

With triethylamine; In N,N-dimethyl-formamide;

Reference yield:

: 1314716-21-6
C₃₈H₄₄O₁₀SSi

: 1314716-30-7
C₅₀H₅₃N₆O₉PS

Guidance literature:: Multi-step reaction with 12 steps

1.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

1.2: 5.5 h / 0 - 55 °C

2.1: potassium carbonate / methanol / 5 h / 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

5.1: pyridine; dmap / 2.5 h / 20 °C

6.1: lithium iodide; ammonium cerium (IV) nitrate / acetonitrile / 3 h / 85 °C

7.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 7 h / 85 °C

7.2: 12 h / 20 °C

8.1: pyridine; dmap / 3 h / 20 °C

9.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C

10.1: triethylamine; trichlorophosphate; 1,2,4-Triazole / acetonitrile / 3 h / 0 - 20 °C

10.2: 2 h

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3.5 h / 20 °C

12.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C

With pyridine; 1H-imidazole; 1,2,4-Triazole; 1-methyl-1H-imidazole; 1H-tetrazole; dmap; bis-triphenylphosphine-palladium(II) chloride; N,O-bis-(trimethylsilyl)-acetamide; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; water; potassium carbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium iodide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1174917-61-3
C₃₇H₃₈N₂O₆Si

: 1314716-30-7
C₅₀H₅₃N₆O₉PS

Guidance literature:: Multi-step reaction with 10 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

3.1: pyridine; dmap / 2.5 h / 20 °C

4.1: lithium iodide; ammonium cerium (IV) nitrate / acetonitrile / 3 h / 85 °C

5.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 7 h / 85 °C

5.2: 12 h / 20 °C

6.1: pyridine; dmap / 3 h / 20 °C

7.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 20 °C

8.1: triethylamine; trichlorophosphate; 1,2,4-Triazole / acetonitrile / 3 h / 0 - 20 °C

8.2: 2 h

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3.5 h / 20 °C

10.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 3 h / 20 °C

With pyridine; 1H-imidazole; 1,2,4-Triazole; 1-methyl-1H-imidazole; 1H-tetrazole; dmap; bis-triphenylphosphine-palladium(II) chloride; ammonium cerium (IV) nitrate; tetrabutyl ammonium fluoride; water; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium iodide; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;