2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine

Base Information

Chemical Name:2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine
CAS No.:1268273-17-1
Molecular Formula:C₂₆H₂₉N₇O₄S
Molecular Weight:535.627
Hs Code.:

Synonyms:2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine

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Chemical Property of 2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine

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Technology Process of 2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine

There total 4 articles about 2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1268273-16-0
5-iodo-4,6-dimethoxy-N,N-bis(4-methoxybenzyl)pyrimidin-2-amine

: 1004-39-3
4,6-diamino-2-mercaptopyrimidine

: 1268273-17-1
2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine

Guidance literature:: With potassium carbonate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; In dimethyl sulfoxide; at 120 ℃; for 16h; Inert atmosphere;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1268273-17-1
2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

1.2: 20 °C

2.1: N-iodo-succinimide / acetonitrile / 1 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline / dimethyl sulfoxide / 16 h / 120 °C / Inert atmosphere

With N-iodo-succinimide; sodium hydride; potassium carbonate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 36315-01-2,256642-28-1
4,6-dimethoxy-2-aminopyrimidine

: 1268273-17-1
2-((2-(bis(4-methoxybenzyl)amino)-4,6-dimethoxypyrimidin-5-yl)thio)pyrimidine-4,6-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

1.2: 20 °C

2.1: N-iodo-succinimide / acetonitrile / 1 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline / dimethyl sulfoxide / 16 h / 120 °C / Inert atmosphere

With N-iodo-succinimide; sodium hydride; potassium carbonate; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;