(6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin

Base Information

Chemical Name:(6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin
CAS No.:124571-93-3
Molecular Formula:C₂₉H₃₀O₆S
Molecular Weight:506.62
Hs Code.:

Synonyms:(6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin

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Chemical Property of (6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin

Chemical Property:

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Technology Process of (6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin

There total 4 articles about (6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 124571-91-1
(6aS,12aS,5'S)-5'-phenylthio-4',5'-dihydrodeguelin

: 124571-93-3
(6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin

Guidance literature:: With sodium tetrahydroborate; In methanol; for 1h; Ambient temperature;

Reference yield:

: 108-98-5
thiophenol

: 124571-93-3
(6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin

Guidance literature:: Multi-step reaction with 4 steps

1: N-chlorosuccinimide / CH₂Cl₂ / Heating

2: CH₂Cl₂ / 2 h / -35 - 20 °C

3: sodium cyanoborohydride / hexamethylphosphoric acid triamide / 2 h / Ambient temperature

4: 90 percent / sodium borohydride / methanol / 1 h / Ambient temperature

With sodium tetrahydroborate; N-chloro-succinimide; sodium cyanoborohydride; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;

Reference yield:

: 124571-92-2
(1S,2R,7aS,13aS)-1-Chloro-9,10-dimethoxy-3,3-dimethyl-2-phenylsulfanyl-2,3,13,13a-tetrahydro-1H,7aH-pyrano[2,3-c;6,5-f']dichromen-7-one

: 124571-93-3
(6aS,12S,12aS,5'S)-12-deoxo-12-hydroxy-5'-phenylthio-4',5'-dihydrodeguelin

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride / hexamethylphosphoric acid triamide / 2 h / Ambient temperature

2: 90 percent / sodium borohydride / methanol / 1 h / Ambient temperature

With sodium tetrahydroborate; sodium cyanoborohydride; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide;