C₉H₉⁽²⁾H₃O₄

Base Information

Chemical Name:C₉H₉⁽²⁾H₃O₄
CAS No.:478703-13-8
Molecular Formula:C₉H₁₂O₄
Molecular Weight:187.168
Hs Code.:

C<sub>9</sub>H<sub>9</sub><sup>(2)</sup>H<sub>3</sub>O<sub>4</sub>

Synonyms:C₉H₉⁽²⁾H₃O₄

Suppliers and Price of C₉H₉⁽²⁾H₃O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₉⁽²⁾H₃O₄

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Technology Process of C₉H₉⁽²⁾H₃O₄

There total 6 articles about C₉H₉⁽²⁾H₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 131135-40-5
2,3-dimethoxy-5-[D₃-methyl]-1,4-benzoquinone

: 478703-13-8
C₉H₉⁽²⁾H₃O₄

Guidance literature:: With sodium dithionite; In diethyl ether; water;
DOI:10.1002/jlcr.587

Reference yield:

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 478703-13-8
C₉H₉⁽²⁾H₃O₄

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / LiAlD₄ / diethyl ether / 4 h / Heating

2: PBr₃; pyridine / diethyl ether / 2 h / 0 - 5 °C

3: 74 percent / LiAlD₄ / diethyl ether / 4 h / Heating

4: 54 percent / 10 percent sulphuric acid; 40 percent acetic acid / acetic acid / 16 h / 25 - 30 °C

5: 64 percent / Na₂S₂O₄ / diethyl ether; H₂O

With pyridine; sodium dithionite; lithium aluminium deuteride; sulfuric acid; phosphorus tribromide; acetic acid; In diethyl ether; water; acetic acid;
DOI:10.1002/jlcr.587

Reference yield:

: 118-41-2
Eudesmic acid

: 478703-13-8
C₉H₉⁽²⁾H₃O₄

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / conc. sulphuric acid / 5 h / Heating

2: 87 percent / LiAlD₄ / diethyl ether / 4 h / Heating

3: PBr₃; pyridine / diethyl ether / 2 h / 0 - 5 °C

4: 74 percent / LiAlD₄ / diethyl ether / 4 h / Heating

5: 54 percent / 10 percent sulphuric acid; 40 percent acetic acid / acetic acid / 16 h / 25 - 30 °C

6: 64 percent / Na₂S₂O₄ / diethyl ether; H₂O

With pyridine; sodium dithionite; lithium aluminium deuteride; sulfuric acid; phosphorus tribromide; acetic acid; In diethyl ether; water; acetic acid;
DOI:10.1002/jlcr.587