C₂₃H₃₀O₇Si

Base Information

Chemical Name:C₂₃H₃₀O₇Si
CAS No.:1293408-38-4
Molecular Formula:C₂₃H₃₀O₇Si
Molecular Weight:446.572
Hs Code.:

C<sub>23</sub>H<sub>30</sub>O<sub>7</sub>Si

Synonyms:C₂₃H₃₀O₇Si

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Chemical Property of C₂₃H₃₀O₇Si

Chemical Property:

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Technology Process of C₂₃H₃₀O₇Si

There total 6 articles about C₂₃H₃₀O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1293408-33-9
N-methoxy-N-methyl-2,3-dimethoxy-4,5-methylenedioxybenzamide

: 177329-71-4
5-Bromo-1-(tert-butyldimethylsilyloxy)-2-methoxybenzene

: 1293408-38-4
C₂₃H₃₀O₇Si

Guidance literature:: 5-Bromo-1-(tert-butyldimethylsilyloxy)-2-methoxybenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

N-methoxy-N-methyl-2,3-dimethoxy-4,5-methylenedioxybenzamide; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.01.124

Reference yield:

: C₁₃H₁₂N₂O₅

: 1293408-38-4
C₂₃H₃₀O₇Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / acetonitrile / 20 h / 40 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With n-butyllithium; triethylamine; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1016/j.bmcl.2011.01.124

Reference yield:

: 484-31-1
dillapiole

: 1293408-38-4
C₂₃H₃₀O₇Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C / Neat (no solvent)

2.1: pyridine; ozone / methanol; chloroform / -15 °C

3.1: urea hydrogen peroxide adduct; sodium hydroxide / methanol; water / 1.5 h / Reflux

4.1: acetonitrile / 0.33 h / 20 °C

5.1: triethylamine / acetonitrile / 20 h / 40 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

6.2: 20 °C / Inert atmosphere

With pyridine; n-butyllithium; tetrabutylammomium bromide; urea hydrogen peroxide adduct; ozone; triethylamine; potassium hydroxide; sodium hydroxide; In tetrahydrofuran; methanol; hexane; chloroform; water; acetonitrile;
DOI:10.1016/j.bmcl.2011.01.124