N₂-(tert-butoxycarbonyl)-N₁-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine

Base Information

• Chemical Name: N₂-(tert-butoxycarbonyl)-N₁-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine
• CAS No.: 1198803-08-5
• Molecular Formula: C₂₈H₃₃N₄O₅P
• Molecular Weight: 536.568

Synonyms:N₂-(tert-butoxycarbonyl)-N₁-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine

Chemical Property of N₂-(tert-butoxycarbonyl)-N₁-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine

Chemical Property:

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Technology Process of N₂-(tert-butoxycarbonyl)-N₁-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine

There total 1 articles about N₂-(tert-butoxycarbonyl)-N₁-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

5-diphenylphosphanylpyrrole-1,2-dicarboxylic-acid 1-tert-butyl ester (1198803-06-3) + tert-butyl carbamimidoylcarbamate (219511-71-4) → N2-(tert-butoxycarbonyl)-N1-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine (1198803-08-5)

Guidance literature:

With 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 20h; Inert atmosphere;

DOI:10.1002/anie.200903620

Reference yield:

N2-(tert-butoxycarbonyl)-N1-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine (1198803-08-5) → N-(5-diphenylphosphanylpyrrole-2-carbonyl)guanidine (1198803-10-9)

Guidance literature:

N₂-(tert-butoxycarbonyl)-N₁-(1-(tert-butoxycarbonyl)-5-diphenylphosphanylpyrrole-2-carbonyl)guanidine; With trifluoroacetic acid; 1,3-Dimethoxybenzene; at 0 - 20 ℃; for 4.5h; Inert atmosphere;

With sodium carbonate; In water; ethyl acetate;

DOI:10.1002/anie.200903620

upstream raw materials:

5-diphenylphosphanylpyrrole-1,2-dicarboxylic-acid 1-tert-butyl ester

tert-butyl carbamimidoylcarbamate

Downstream raw materials:

N-(5-diphenylphosphanylpyrrole-2-carbonyl)guanidine

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