C₃₄H₃₄O₄

Base Information

Chemical Name:C₃₄H₃₄O₄
CAS No.:226225-96-3
Molecular Formula:C₃₄H₃₄O₄
Molecular Weight:506.642
Hs Code.:

C<sub>34</sub>H<sub>34</sub>O<sub>4</sub>

Synonyms:C₃₄H₃₄O₄

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Chemical Property of C₃₄H₃₄O₄

Chemical Property:

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Technology Process of C₃₄H₃₄O₄

There total 5 articles about C₃₄H₃₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 226225-95-2
C₃₆H₃₈O₄

: 226225-96-3
C₃₄H₃₄O₄

Guidance literature:: 2,6-diisopropylphenylimide neophylidenemolybdenum(IV) bis(he; xafluoro-t-butoxide); In dichloromethane; at 20 ℃; for 18h;
DOI:10.1515/znb-1999-0422

Reference yield:

: 160549-10-0
2,3,5-tri-O-benzyl-D-arabinofuranose

: 226225-96-3
C₃₄H₃₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: BuLi / tetrahydrofuran; hexane / 1.5 h / 0 - 20 °C

1.2: 87 percent / tetrahydrofuran; hexane

2.1: 90 percent / (COCl)2; DMSO; NEt₃ / CH₂Cl₂ / 0.42 h / -78 - 0 °C

3.1: 92 percent / tetrahydrofuran / -78 - 0 °C

4.1: NaH / dimethylformamide / 0 °C

4.2: 98 percent / Bu₄NI / dimethylformamide / 0.5 h

5.1: 87 percent / 2,6-diisopropylphenylimide neophylidenemolybdenum(IV) bis(he; xafluoro-t-butoxide) / CH₂Cl₂ / 18 h / 20 °C

With n-butyllithium; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; triethylamine; 2,6-diisopropylphenylimide neophylidenemolybdenum(IV) bis(he; xafluoro-t-butoxide); In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 1.1: Elimination / 1.2: Condensation / 2.1: Oxidation / 3.1: Grignard reaction / 4.1: Metallation / 4.2: Substitution / 5.1: Cyclization;
DOI:10.1515/znb-1999-0422

Reference yield:

: 102208-53-7
(3R,4R,5R)-5-hydroxy-3,4,6-tribenzyloxy-1-hexene

: 226225-96-3
C₃₄H₃₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: 90 percent / (COCl)2; DMSO; NEt₃ / CH₂Cl₂ / 0.42 h / -78 - 0 °C

2.1: 92 percent / tetrahydrofuran / -78 - 0 °C

3.1: NaH / dimethylformamide / 0 °C

3.2: 98 percent / Bu₄NI / dimethylformamide / 0.5 h

4.1: 87 percent / 2,6-diisopropylphenylimide neophylidenemolybdenum(IV) bis(he; xafluoro-t-butoxide) / CH₂Cl₂ / 18 h / 20 °C

With oxalyl dichloride; sodium hydride; dimethyl sulfoxide; triethylamine; 2,6-diisopropylphenylimide neophylidenemolybdenum(IV) bis(he; xafluoro-t-butoxide); In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.1: Oxidation / 2.1: Grignard reaction / 3.1: Metallation / 3.2: Substitution / 4.1: Cyclization;
DOI:10.1515/znb-1999-0422