decamethylferrocenium tetrakis(pentafluorophenyl)borate

Base Information

• Chemical Name: decamethylferrocenium tetrakis(pentafluorophenyl)borate
• CAS No.: 135348-60-6
• Molecular Formula: C₂₀H₃₀Fe*C₂₄BF₂₀
• Molecular Weight: 1005.35

Synonyms:decamethylferrocenium tetrakis(pentafluorophenyl)borate

Chemical Property of decamethylferrocenium tetrakis(pentafluorophenyl)borate

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Technology Process of decamethylferrocenium tetrakis(pentafluorophenyl)borate

There total 4 articles about decamethylferrocenium tetrakis(pentafluorophenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.12%

bis(pentamethylcyclopentadienyl)iron(II) (12126-50-0) + tetrakis(acetonitrile)silver(I) tetrakis(pentafluorophenyl)borate (848737-65-5) → decamethylferrocenium tetrakis(pentafluorophenyl)borate (135348-60-6)

Guidance literature:

In 2-methyltetrahydrofuran; at 20 ℃; for 1h; Glovebox; Inert atmosphere; Darkness;

DOI:10.1039/d1dt01192h

Reference yield: 76.0%

bis(pentamethylcyclopentadienyl)iron(II) (12126-50-0) + potassium tetrakis(pentafluorophenyl)borate → decamethylferrocenium tetrakis(pentafluorophenyl)borate (135348-60-6)

Guidance literature:

With silver nitrate; In acetonitrile; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1021/jacs.9b00795 DOI:10.1021/jacs.9b00795

Reference yield: 40.0%

hydrogen tetrakis(pentafluorophenyl)borate + bis(pentamethylcyclopentadienyl)iron(II) (12126-50-0) → decamethylferrocenium tetrakis(pentafluorophenyl)borate (135348-60-6) + dihydrogen peroxide (7722-84-1)

Guidance literature:

With O₂; In 1,2-dichloro-ethane; H₂O; shaken;

DOI:10.1039/b926963k

upstream raw materials:

bis(pentamethylcyclopentadienyl)iron(II)

tetrakis(acetonitrile)silver(I) tetrakis(pentafluorophenyl)borate

Downstream raw materials:

Ti(CH(C(CH₃)NC₆H₃(CH(CH₃)2)2)2)(HNC₆H₃(CH(CH₃)2)2)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=Ti(CH(C(CH₃)NC₆H₃(C₃H₇)2)2)(HNC₆H₃(C₃H₇)2)2B(C₆F₅)4

(C₆H₃(CH(CH₃)2)2NCCH₃CHCCH₃NC₆H₃(CH(CH₃)2)2)Ti(CH₂C(CH₃)3)2⁽¹⁺⁾*B(C₆F₅)4^(1-)=((C₆H₃(C₃H₇)2NCCH₃)2CH)Ti(CH₂C₄H₉)2B(C₆F₅)4

[(N(CH₂CH₂NSi(t-Bu)Me₂)3)U(V)(phenylacetylide)]⁽¹⁺⁾ C₃₂H₆₂N₄Si₃U⁽¹⁺⁾, monoclinic

bis(pentamethylcyclopentadienyl)iron(II)

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