(S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine

Base Information

Chemical Name:(S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine
CAS No.:219598-58-0
Molecular Formula:C₁₃H₁₅NO₃
Molecular Weight:233.267
Hs Code.:

Synonyms:(S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine

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Chemical Property of (S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine

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Technology Process of (S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine

There total 2 articles about (S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 219598-57-9
(S)-2-hydroxymethyl-N,O-bisbenzoylformyl pyrrolidine

: 219598-58-0
(S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(98)00914-4

Reference yield:

: 23356-96-9
(S)-1-Pyrrolidin-2-yl-methanol

: 219598-58-0
(S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / Et₃N, DMAP / CH₂Cl₂ / 6 h / Ambient temperature

2: 85 percent / NaOH / tetrahydrofuran; H₂O / 2 h / Ambient temperature

With dmap; sodium hydroxide; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0040-4020(98)00914-4

Reference yield:

: 219598-58-0
(S)-2-hydroxymethyl-N-benzoylformyl pyrrolidine

: 611-71-2
(R)-Mandelic Acid

Guidance literature:: Multi-step reaction with 2 steps

1: KBH₄ / methanol / 10 h / 0 °C

2: 95 percent / H₂SO₄ / H₂O / 0.5 h / 90 °C

With potassium borohydride; sulfuric acid; In methanol; water;
DOI:10.1016/S0040-4020(98)00914-4