N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate

Base Information

Chemical Name:N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate
CAS No.:1350711-74-8
Molecular Formula:C₁₂H₂₃N*C₁₃H₁₃BrO₃
Molecular Weight:478.47
Hs Code.:

Synonyms:N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate

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Chemical Property of N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate

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Technology Process of N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate

There total 4 articles about N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350711-72-6
(4R)-4-benzyl-3-{[(1R,2R)-2-(4-bromophenyl)-4-oxocyclohexyl]carbonyl}-1,3-oxazolidin-2-one

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 1350711-74-8
N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate

Guidance literature:: (4R)-4-benzyl-3-{[(1R,2R)-2-(4-bromophenyl)-4-oxocyclohexyl]carbonyl}-1,3-oxazolidin-2-one; With 2,2-Dimethyl-1,3-propanediol; toluene-4-sulfonic acid; In toluene; for 3h; Reflux;

With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃;

N-cyclohexyl-cyclohexanamine;

Reference yield:

: 1200-07-3,5676-63-1,17916-60-8
trans-4-bromocinnamic acid

: 1350711-74-8
N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 5 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran / 0.58 h / -65 °C

2.2: 0.75 h / -65 °C

3.1: diethylaluminium chloride / dichloromethane / 0 - 20 °C

4.1: 2,2-Dimethyl-1,3-propanediol / toluene-4-sulfonic acid / toluene / 3 h / Reflux

4.2: 0 - 20 °C

With n-butyllithium; oxalyl dichloride; diethylaluminium chloride; 2,2-Dimethyl-1,3-propanediol; toluene-4-sulfonic acid; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 27465-66-3,13565-09-8
4-bromocinnamoyl chloride

: 1350711-74-8
N-cyclohexylcyclohexanaminium (1R,2R)-2-(4-bromophenyl)-4-oxocyclohexane-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 0.58 h / -65 °C

1.2: 0.75 h / -65 °C

2.1: diethylaluminium chloride / dichloromethane / 0 - 20 °C

3.1: 2,2-Dimethyl-1,3-propanediol / toluene-4-sulfonic acid / toluene / 3 h / Reflux

3.2: 0 - 20 °C

With n-butyllithium; diethylaluminium chloride; 2,2-Dimethyl-1,3-propanediol; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; toluene;