7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

Base Information

Chemical Name:7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine
CAS No.:1319732-02-9
Molecular Formula:C₁₉H₂₂ClN₃O₂
Molecular Weight:359.856
Hs Code.:

Synonyms:7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

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Chemical Property of 7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

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Technology Process of 7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

There total 3 articles about 7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-52-1
1,4-dibromo-butane

: 1319731-99-1
2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

: 124-41-4
sodium methylate

: 1319732-03-0
9-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

: 1319732-02-9
7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

Guidance literature:: 1,4-dibromo-butane; 2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

sodium methylate; In methanol; at 45 ℃; for 16h;
DOI:10.1016/j.bmcl.2011.05.093

Reference yield:

: 579486-60-5
4,6-dichloro-2-methyl-1H-imidazo[4,5-c]pyridine

: 1319732-02-9
7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium / 120 °C

2.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 20 °C

2.2: 16 h / 45 °C

With sodium; tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.05.093

Reference yield:

: 3,4-diamino-2,6-dichloropyridine dihydrochloride

: 1319732-02-9
7-(4-methoxybutyl)-2-chloro-6-benzyloxy-8-methylimidazo[4,5-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphoric acid / 16 h / 80 °C

2.1: sodium / 120 °C

3.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 20 °C

3.2: 16 h / 45 °C

With phosphoric acid; sodium; tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.05.093