N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide

Base Information

Chemical Name:N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide
CAS No.:1201663-20-8
Molecular Formula:C₂₇H₂₄Cl₂N₂O₃S
Molecular Weight:527.471
Hs Code.:

Synonyms:N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide

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Chemical Property of N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide

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Technology Process of N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide

There total 3 articles about N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1201660-72-1
tert-butyl 3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzylcarbamate

: 1201663-20-8
N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide

Guidance literature:: tert-butyl 3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzylcarbamate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

With sodium hydrogencarbonate; In water;

Reference yield:

: 3218-36-8
4-Phenylbenzaldehyde

: 1201663-20-8
N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane; N,N-dimethyl-formamide / 0.67 h / 20 °C

1.2: 3 h / 20 °C

2.1: triethylamine / dichloromethane / 1.5 h / Cooling

3.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 108467-99-8
1-(N-Boc-aminomethyl)-3-(aminomethyl)benzene

: 1201663-20-8
N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane; N,N-dimethyl-formamide / 0.67 h / 20 °C

1.2: 3 h / 20 °C

2.1: triethylamine / dichloromethane / 1.5 h / Cooling

3.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;