5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid

Base Information

Chemical Name:5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid
CAS No.:1201660-66-3
Molecular Formula:C₃₅H₃₀Cl₂N₂O₇S₂
Molecular Weight:725.67
Hs Code.:

Synonyms:5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid

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Chemical Property of 5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid

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Technology Process of 5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid

There total 5 articles about 5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.1%

: 1201663-20-8
N-(3-(aminomethyl)benzyl)-N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxybenzenesulfonamide

: 89001-57-0
5-(chlorosulfonyl)-2-methylbenzenecarboxylic acid

: 1201660-66-3
5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1.16667h;

Reference yield:

: 1201663-19-5
tert-butyl 3-((biphenyl-4-ylmethylamino)methyl)benzylcarbamate

: 1201660-66-3
5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 1.5 h / Cooling

2: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

3: triethylamine / dichloromethane / 1.17 h / 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 1201660-72-1
tert-butyl 3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzylcarbamate

: 1201660-66-3
5-(N-(3-((N-(biphenyl-4-ylmethyl)-3,5-dichloro-2-hydroxyphenylsulfonamido)methyl)benzyl)sulfamoyl)-2-methyl benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

2: triethylamine / dichloromethane / 1.17 h / 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;