2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride

Base Information

Chemical Name:2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride
CAS No.:78335-93-0
Molecular Formula:C₈H₈Cl₃NO₂*ClH
Molecular Weight:292.977
Hs Code.:

Synonyms:2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride

Chemical Property:

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Technology Process of 2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride

There total 3 articles about 2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78335-96-3
2-(1-hydroxy-2-nitroethyl)3,4,6-trichlorophenol

: 78335-93-0
2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; Rh on carbon; for 48h; under 1654.9 Torr;
DOI:10.1021/jm00141a009

Reference yield:

: 23602-65-5
2,3,5-trichloro-6-hydroxybenzaldehyde

: 78335-93-0
2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 10percent aq. NaOH / dimethylformamide / 2 h / Ambient temperature

2: 1.15 g / 6N HCl, H₂ / 5percent Rh/C / 48 h / 1654.9 Torr

With hydrogenchloride; sodium hydroxide; hydrogen; Rh on carbon; In N,N-dimethyl-formamide;
DOI:10.1021/jm00141a009

Reference yield:

: 95-95-4
2,4,5-trichlorophenol

: 78335-93-0
2-(2-amino-1-hydroxyethyl)-3,4,6-trichlorophenol hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 19 percent / Ca(OH)2, Na₂CO₃ / H₂O / 16 h / 65 °C

2: 73 percent / 10percent aq. NaOH / dimethylformamide / 2 h / Ambient temperature

3: 1.15 g / 6N HCl, H₂ / 5percent Rh/C / 48 h / 1654.9 Torr

With hydrogenchloride; calcium hydroxide; sodium hydroxide; hydrogen; sodium carbonate; Rh on carbon; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm00141a009