(Z)-14-tricosenyl tosylate

Base Information

Chemical Name:(Z)-14-tricosenyl tosylate
CAS No.:159627-65-3
Molecular Formula:C₃₀H₅₂O₃S
Molecular Weight:492.807
Hs Code.:

Synonyms:(Z)-14-tricosenyl tosylate

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Chemical Property of (Z)-14-tricosenyl tosylate

Chemical Property:

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Technology Process of (Z)-14-tricosenyl tosylate

There total 8 articles about (Z)-14-tricosenyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 50995-26-1
(Z)-14-tricosen-1-ol

: 98-59-9
p-toluenesulfonyl chloride

: 159627-65-3
(Z)-14-tricosenyl tosylate

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 6h; Ambient temperature;

Reference yield:

: 13362-52-2
1,13-tridecanediol

: 159627-65-3
(Z)-14-tricosenyl tosylate

Guidance literature:: Multi-step reaction with 7 steps

1: 72 percent / 48percent HBr / benzene / 36 h / Heating

2: 98 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 4 h / Ambient temperature

3: 91 percent / xylene; tetrahydrofuran; hexamethylphosphoric acid triamide / 36 h / Ambient temperature

4: 1.) 1.63N butyllithium / 1.) hexane, THF, -50 deg C, 30 min; 0 deg C, 30 min, 2.) hexane, THF, HMPA, -50 deg C, 30 min; 0 deg C, 2 h

5: 93 percent / p-toluenesulfonic acid monohydrate / methanol / 2 h / Ambient temperature

6: H₂, quinoline / Lindlar palladium catalyst / hexane / 20.5 h / Ambient temperature

7: 98 percent / triethylamine, (4-dimethylamino)pyridine / CH₂Cl₂ / 6 h / Ambient temperature

With quinoline; dmap; n-butyllithium; hydrogen bromide; hydrogen; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; triethylamine; Lindlar's catalyst; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; xylene; benzene;

Reference yield:

: 116754-58-6
13-bromo-1-tridecylalcohol

: 159627-65-3
(Z)-14-tricosenyl tosylate

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 4 h / Ambient temperature

2: 91 percent / xylene; tetrahydrofuran; hexamethylphosphoric acid triamide / 36 h / Ambient temperature

3: 1.) 1.63N butyllithium / 1.) hexane, THF, -50 deg C, 30 min; 0 deg C, 30 min, 2.) hexane, THF, HMPA, -50 deg C, 30 min; 0 deg C, 2 h

4: 93 percent / p-toluenesulfonic acid monohydrate / methanol / 2 h / Ambient temperature

5: H₂, quinoline / Lindlar palladium catalyst / hexane / 20.5 h / Ambient temperature

6: 98 percent / triethylamine, (4-dimethylamino)pyridine / CH₂Cl₂ / 6 h / Ambient temperature

With quinoline; dmap; n-butyllithium; hydrogen; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; triethylamine; Lindlar's catalyst; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; xylene;