methyl 5-O-benzyl-2,6-dideoxy-α-L-lyxo-hexofuranoside

Base Information

Chemical Name:methyl 5-O-benzyl-2,6-dideoxy-α-L-lyxo-hexofuranoside
CAS No.:78841-76-6
Molecular Formula:C₁₄H₂₀O₄
Molecular Weight:252.31
Hs Code.:

Synonyms:methyl 5-O-benzyl-2,6-dideoxy-α-L-lyxo-hexofuranoside

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Chemical Property of methyl 5-O-benzyl-2,6-dideoxy-α-L-lyxo-hexofuranoside

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Technology Process of methyl 5-O-benzyl-2,6-dideoxy-α-L-lyxo-hexofuranoside

There total 36 articles about methyl 5-O-benzyl-2,6-dideoxy-α-L-lyxo-hexofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 78841-75-5
methyl 2,3-anhydro-5-O-benzyl-α-L-gulofuranoside

: 78841-76-6
methyl 5-O-benzyl-2,6-dideoxy-α-L-lyxo-hexofuranoside

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -10 ℃; for 0.5h;
DOI:10.1016/S0008-6215(00)80395-X

Reference yield: 65.0%

: 111651-73-1,111766-78-0
(2S,3R)-2-((R)-1-Benzyloxy-2,2-bis-ethylsulfanyl-ethyl)-5-methoxy-tetrahydro-furan-3-ol

: 76235-03-5,78841-76-6,111651-74-2,130169-86-7,130169-88-9,130169-93-6,130169-94-7,130169-97-0,130203-44-0,130203-46-2
(2S,3R)-2-((S)-1-Benzyloxy-ethyl)-5-methoxy-tetrahydro-furan-3-ol

Guidance literature:: With hydrogen; nickel; for 48h;
DOI:10.1016/S0040-4039(00)95361-9

Reference yield:

: 7057-10-5
1,2-O-isopropylidene-α-D-5-deoxyglucurono-6,3-lactone

: 76235-03-5,78841-76-6,111651-74-2,130169-86-7,130169-88-9,130169-93-6,130169-94-7,130169-97-0,130203-44-0,130203-46-2
(2S,3R)-2-((S)-1-Benzyloxy-ethyl)-5-methoxy-tetrahydro-furan-3-ol

Guidance literature:: Multi-step reaction with 6 steps

1: Amberlite IR 120 (H) resin / Heating

2: 54 percent / silver oxide / benzene

3: conc. HCl

4: 60 percent / DIBAL / CH₂Cl₂ / -78 °C

5: IR 120 resin / Heating

6: 65 percent / hydrogen / Raney nickel / 48 h

With hydrogenchloride; Amberlite IR 120 (H) resin; IR 120 resin; hydrogen; diisobutylaluminium hydride; silver(l) oxide; nickel; In dichloromethane; benzene;
DOI:10.1016/S0040-4039(00)95361-9