benzyl N-pyridin-3-ylcarbamate

Base Information

Chemical Name:benzyl N-pyridin-3-ylcarbamate
CAS No.:170839-31-3
Molecular Formula:C₁₃H₁₂N₂O₂
Molecular Weight:228.25
Hs Code.:
DSSTox Substance ID:DTXSID701331651
ChEMBL ID:CHEMBL1595616
Mol file:170839-31-3.mol

Synonyms:benzyl N-pyridin-3-ylcarbamate;170839-31-3;BENZYL N-(PYRIDIN-3-YL)CARBAMATE;Carbamic acid, 3-pyridinyl-, phenylmethyl ester (9CI);3-Carbobenzyloxyaminopyridine;Pyridin-3-yl-carbamic acid benzyl ester;Benzyl 3-pyridinylcarbamate;Oprea1_427180;MLS001208699;SCHEMBL968903;CHEMBL1595616;WKCRLJFVJSENNX-UHFFFAOYSA-N;DTXSID701331651;HMS2846N24;AKOS000670231;SMR000518763;FT-0732692;F70561;SR-01000491672;SR-01000491672-1

Suppliers and Price of benzyl N-pyridin-3-ylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of benzyl N-pyridin-3-ylcarbamate

Chemical Property:

Melting Point:164-165 °C
Boiling Point:345.9±25.0 °C(Predicted)
PKA:12.87±0.70(Predicted)
Density:1.248±0.06 g/cm3(Predicted)
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:228.089877630
Heavy Atom Count:17
Complexity:240

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC(=O)NC2=CN=CC=C2

Technology Process of benzyl N-pyridin-3-ylcarbamate

There total 4 articles about benzyl N-pyridin-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 462-08-8
pyridin-3-ylamine

: 124-38-9,18923-20-1
carbon dioxide

: 100-44-7
benzyl chloride

: 170839-31-3
benzyl N-(pyridin-3-yl)carbamate

Guidance literature:: pyridin-3-ylamine; carbon dioxide; With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 23 ℃; for 1h;

benzyl chloride; In N,N-dimethyl-formamide; at 23 ℃; for 12h;
DOI:10.1016/S0040-4020(02)00286-7

Reference yield: 88.0%

: 626-55-1,163928-56-1
3-Bromopyridine

: 621-84-1
O-benzyl carbamate

: 170839-31-3
benzyl N-(pyridin-3-yl)carbamate

Guidance literature:: With ?di-tert-butyl(2,2-diphenyl-1-methyl-1-cyclopropyl)phosphine; bis(η3-allyl-μ-chloropalladium(II)); sodium t-butanolate; In water; at 50 ℃; for 24h; Inert atmosphere; Green chemistry;
DOI:10.1039/c3gc42188k