(S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate

Base Information

Chemical Name:(S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate
CAS No.:863455-75-8
Molecular Formula:C₂₃H₂₇N₃O₃
Molecular Weight:393.486
Hs Code.:

Synonyms:(S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate

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Chemical Property of (S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate

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Technology Process of (S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate

There total 3 articles about (S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95899-01-7
(2-methoxyphenyl)(pyridine-2-yl)methanamine

: 863455-75-8
(S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C

2: pyridine; trichlorophosphate / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

With pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trichlorophosphate; In dichloromethane;
DOI:10.1089/adt.2016.708

Reference yield:

: 16750-63-3
2-methoxyphenylmagnesium bromide

: 863455-75-8
(S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene; tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere

1.2: 14 h / 20 °C / Inert atmosphere

2.1: benzotriazol-1-ol; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C

3.1: pyridine; trichlorophosphate / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

With pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1089/adt.2016.708

Reference yield:

: 100-70-9,1232006-36-8
2-Cyanopyridine

: 863455-75-8
(S)-tert-butyl 2-(1-(2-methoxyphenyl)imidazo[1,5-a]pyridine-3-yl)pyrrolidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene; tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere

1.2: 14 h / 20 °C / Inert atmosphere

2.1: benzotriazol-1-ol; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 20 °C

3.1: pyridine; trichlorophosphate / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

With pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1089/adt.2016.708