2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone

Base Information

Chemical Name:2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone
CAS No.:100448-56-4
Molecular Formula:C₁₅H₁₂ClF₃N₄O₃S
Molecular Weight:420.799
Hs Code.:

2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde <m-(trifluoromethyl)phenyl>hydrazone

Synonyms:2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone

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Chemical Property of 2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone

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Technology Process of 2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone

There total 3 articles about 2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 100448-45-1
5-chloro-3-hydroxy-6-sulfamoylphthalimidine

: 368-78-5
3-(trifluoromethyl)phenylhydrazine

: 100448-56-4
2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone

Guidance literature:: In ethanol; water; at 85 ℃; for 6h;
DOI:10.1021/jm00156a011

Reference yield:

: 2736-23-4
2,4-dichloro-5-sulfamoylbenzoic acid

: 100448-56-4
2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / dimethylformamide / 2 h / 160 °C

2: 34 percent / AcOH, Zn / methanol / 6 h / 45 °C

3: 54 percent / ethanol; H₂O / 6 h / 85 °C

With acetic acid; zinc; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00156a011

Reference yield:

: 3861-99-2
4-chloro-5-sulfamoylphthalimide

: 100448-56-4
2-(aminocarbonyl)-5-chloro-4-sulfamoylbenzaldehyde hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / AcOH, Zn / methanol / 6 h / 45 °C

2: 54 percent / ethanol; H₂O / 6 h / 85 °C

With acetic acid; zinc; In methanol; ethanol; water;
DOI:10.1021/jm00156a011